In a recent study, a mixture of poly 2-(4-fluorophenyl)-2-oxoethyl-2-methylprop-2-enoate (PFPAMA) and PVA was first prepared and characterized using the hydrothermal method. Copper (II) oxide nanoparticles (CuO NPs) prepared by solution plasma process (SPP) were hydrothermally incorporated into the PVA-PFPAMA blend at 3 %, 5 %, and 7 %. FTIR spectroscopy was used to identify the functional groups of the obtained materials. Morphological and structural analysis of the materials was investigated by scanning electron microscopy (SEM), X-ray diffraction (XRD), and atomic force microscopy (AFM).